I am working on my Safety Protocol and Workflow a Google Doc - click here for Safety Data Sheets, protocol and notes of my experiments thus far here:
Lye
-
‘Lessive’ in French MS, in Cotgrave, ‘lexive’ is described as “lye (wherewith linnen is cleansed;) also, a bucke of (linnen) clothes”
-
Alkalized water, primarily that made by the lixiviation of vegetable ashes, but also applied (esp. with prefixed word as in soap-lye, soda-lye) to any strong alkaline solution, esp. one used for the purpose of washing. †Also water of lye.
"lye, n.1". OED Online. March 2016. Oxford University Press.
http://www.oed.com/view/Entry/111578?rskey=TpocRZ&result=1&isAdvanced=false
(accessed March 20, 2016).
Research lyes as mordants
Litharge or White Lead?
The french term in the MS is 'litharge'
So is this recipe using white lead or litharge - and if litharge, is it yellow lead or red lead?
Thid term is only used once again in the manuscript in the below recipe:
32v
VitrierIls nont poinct linvention de faire un rouge parfaict en besoigne quil fault recuire Touteffois essaye le rouge dallemaigne qui est rouge descaille Ils font leur rouge commun avecq de la sanguineestain de glacerocaille litharge & un peu descaille de fer. Ledict rouge se charge dun coste & daultre du verre affin quil aye plus de couleur sil nestoit charge que dun coste il seroit trop orange paste
Glassmakers
They have no way to produce a perfect red that needs to be annealed. Try, however, the German red which is scaled red. They produce their ordinary red with some sanguine iced pewter, lead rocks, and some iron file dust. This red is to be applied on both sides of the glass< because it is more colourful. If it were applied on one side only it would look pastel orange.
Litharge is Lead Oxide, whereas White Lead is a basic lead carbonate.
Question: is this an unusual recipe, but one suitable given he is in a metal workshop? Is this about the availability of goods, and the trade and identity of the author practitioner (in the same manner as the hourglass sand experiment?)
Litharge in the OED:
a.
Protoxide of lead (PbO) prepared by exposing melted lead to a current of air. †Also
litharge of lead
.
1322 in 23/20
Litarge
4
d
. per lb.
c
1386
Chaucer
222
Oure grounden
litarge
eek in the P[o]rfurie.
1477
T. Norton
Ordinall of Alchimy
iii, in E. Ashmole (1652) 41
Then we name it our grounde
Litharge
.
1563
T. Galeiv. ii.
f. 48
v
,
Take
Litarge
of leide in fyne pouder.
1674
J. Ray
Smelting Silver
in 114
When the furnace is come to a true temper of heat the Lead converted into
Litharge
is cast off.
1707 tr. P. Le Lorrain de Vallemont 325
Lead being..burnt into
Litargie
, retakes also its first Form..if a Lixiviate Salt be..applied to it.
1758
A. Reid
tr. P. J. Macquer I. 389
Pure Lead, being exposed to a strong fire without any additament, turns to
Litharge
.
1860
G. W. S. Piesse
155
Put a few grains of
litharge
before the blowpipe flame.
(Hide quotations)
†
b.
litharge of gold
: a name given to litharge when coloured red by mixture of red lead.
litharge of silver
: a name given to it as being a by-product in the separation of silver from lead.
litharge of bismuth
: ? a similar product obtained by the oxidation of bismuth.
Obs.
c
1400 99
Take..
litarge of gold
, litarge of siluir g. viii.
1578
H. Lyte
tr. R. Dodoens
vi.
lxxxvii. 771
To be pound with the lytarge of sylver and frankencense.
1597
J. Gerardii.
269
The iuice mixed with oile of roses, ceruse, and
littarge of golde
, and applied [etc.].
1601
P. Holland
tr. Pliny I. 304
The very root of the right Nard..is mingled..with Litharge of siluer, Antimony, or the rind of Cyperus.
1639
T. de Grayii.
ix. 208
Take lyturgy of Gold, and lyturgy of Silver.. Mixe well the lyturgys.
1718
J. Quincyii.
xii. 213
Lethargyrus Auri
,
Letharge of Gold
. It generally is call'd thus for its Colour sake.
1728
E. Chambers
(at cited word),
Artificial Litharge is of two Kinds, viz. that of Gold, and that of Silver; or rather 'tis the same, with this difference, that the one having undergone a greater Degree of Fire than the other has occasioned different Colours, and thence different Names.
1796
R. Kirwan
(ed. 2) II. 489
Litharge of Bismuth
.
(Hide quotations)
†
2.
Used as equivalent to
white lead
or
red lead
(see
lead n.1 2
).
1551
W. Turner
sig. M j,
The iuice of Coriandre with whyte lede or
lythurgyry
and vinegre.
1660
J. Howell
sig. H h h
v
,
Litargie
, or white Lead.
1683
J. Pettus
(1686)
i.
26
Of these pibble-stones take one part, and half a part of red
Littorage
or Littarge..and hete it well.
1796
R. Kirwan
(ed. 2) II. 368
Litharge
or Red Lead.
1800 tr. E. J. B. Bouillon-Lagrange II. 64
If you expose to heat in a crucible red oxide of lead or
litharge
.
Amsterdam student work in Drive Student Files
Fall 2015 files by Yuan Yi and Cindy Kok